Determination of water content in tea samples of Cymbopogon citratus S., Matricaria recutita L., Mentha spp. and Pimpinella anisum L. through Gravimetric and Thermogravimetric methods

Authors

  • Pedro Fantoni Maciel Pharmaceutical Quality Control Lab from the Faculty of Pharmacy at Federal University of Rio Grande do Sul image/svg+xml
  • Martin Steppe Pharmaceutical Quality Control Lab from the Faculty of Pharmacy at Federal University of Rio Grande do Sul image/svg+xml

DOI:

https://doi.org/10.22456/2527-2616.79223

Keywords:

Humidity, Teas, Loss on Drying, Thermogravimetry, Infrared

Abstract

The excess of humidity in materials of plant origin allows the action of enzymes, which can cause degradation of chemical components and enable fungi and bacteria development. The humidity determination is one of the most important and most used measurements in food analysis, as it is tightly related to food quality, stability and composition. Teas are among humanity’s most popular and most broadly diffused drinks, being the most common form of phytoterapeutical products and a natural source of chemical substances with activity against a broad variety of ailments. Humidity determination in teas of Cymbopogon citratus S., Matricaria recutita L., Mentha spp. and Pimpinella anisum L was performed through pharmacopoeia-standards gravimetric analysis, drying by infrared radiation and thermogravimetry, and the results obtained by each method were compared. All humidity indexes obtained were in accordance with the currently available official specifications. Water content values obtained by the pharmacopoeia-standards assay, infrared radiation assay and thermogravimetry presented statistical difference between them, due to the methods’ technical features or the utilized materials’ physical characteristics; still the thermogravimetry and the infrared radiation assay were the methods that presented the least statistical difference between their results. The pharmacopoeia-standards method presented itself as the more adequate method for the determination of water content in materials of plant origin, like teas.

Downloads

Download data is not yet available.

References

Araújo AAS, Mercuri LP, Seixas SRS, Storpirtis S, Matos JR. Determinação dos teores de umidade e cinzas de amostras comerciais de guaraná utilizando métodos convencionais e análise térmica. Braz J Pharm Sci. 2006;42 (1):269-277

Awang DVC. Tyler’s Herbs of Choice: The Therapeutic Use of Phytomedicinals. 3 rd. ed. Boca Raton: CRC Press; 2009.

Barnes J, Anderson LA, Phillipson JD. Herbal Medicines. 3rd. ed. London: Pharmaceutical Press; 2007.

Borges DB, Farias MR, Simões CMO, Schenkel EP. Comparação das metodologias da Farmacopéia Brasileira para determinação de água em matériasprimas vegetais, e validação da determinação de água em analisador de umidade para Calendula officinalis L., Foeniculum vulgare Miller, Maytenus ilicifolia Mart. ex. Reissek e Passiflora alata Curtis. Braz. J Pharmacog. 2005;15(3):229-236.

Bradley Jr. RL. Moisture and Total Solids Analysis. In: Nielsen SS. Food Analysis. London: Springer; 2000.

Brazil. Agência Nacional de Vigilância Sanitária. Farmacopeia Brasileira. 5ª ed. Brasília, 2010.

Cecchi HM. Fundamentos Teóricos e Práticos em Análise de Alimentos. Campinas: Unicamp; 2003.

Farias MR. Avaliação da qualidade de matérias-primas vegetais. In: Simões CMO. Farmacognosia: da Planta ao Medicamento. Porto Alegre / Florianópolis: Ed. Universidade - UFRGS/ Ed. da UFSC; 2002.

Fetrow CW, Avila JR. Professional’s Handbook of Complementary & Alternative Medicines. Philadelphia: Lippincott

Williams & Wilkins; 2000.

France. Council of Europe. European Pharmacopoeia. 8ª Edição. Estrasburgo, 2014.

Frazier RA. Food Chemistry – Water in Foods. In: Campbell-Platt G. Food Science and Technology. Chicester: Wiley-Blackwell; 2009.

Instituto Adolfo Lutz. Secretaria De Estado Da Saúde. Métodos FísicoQuímicos para Análise de Alimentos. 1st. ed. Sao Paulo; 2008.

Isengard HD. Rapid Water Determination in Foodstuffs. Trends Food Sci Technol. 1995;6(5):155-162.

Isengard HD, Präger H. Water determination in products with high sugar content by infrared drying. Food Chem. 2003;82(1):161-167.

Isengard HD, Breithaupt D. Food Analysis – Instrumental Methods. In: Campbell-Platt G. Food Science and Technology. Chicester: Wiley-Blackwell, 2009.

Komatsu H, Yoshii K, Okada S. Application of Thermogravimetry to Water-Content Determinations of Drugs. Chem Pharm Bull. 1994;42(8):1631- 1635.

Materazzi S, De Angelis Curtis S, Sagone F, Quaglia GB, Bucarelli FM, Aquili S, Paolesse R, Vecchio S, Curini R, D’ascenzo G. Thermal Analysis and Food Quality: The possibility to qualify the pasta processing. J Therm Anal Calorim. 2005;80(2):465-467.

Rankell AS, Lieberman HA, Schiffman RF. Drying. In: Lachman L. The Theory and Practice of Industrial Pharmacy. Philadelphia: Lea & Febiger, 1986.

Thomas LC, Schmidt SJ. Thermal Analysis. In: Nielsen SS. Food Analysis. London: Springer, 2000.

Trevisanato SI, Young-In K. Tea and Health. Nutr Rev. 2000;58(1):1-10.

Downloads

Published

28-12-2017 — Updated on 10-03-2026

Versions

How to Cite

Fantoni Maciel, P., & Steppe, M. (2026). Determination of water content in tea samples of Cymbopogon citratus S., Matricaria recutita L., Mentha spp. and Pimpinella anisum L. through Gravimetric and Thermogravimetric methods . Drug Analytical Research, 1(2), 53–60. https://doi.org/10.22456/2527-2616.79223 (Original work published December 28, 2017)

Issue

Section

ORIGINAL ARTICLES